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6-Methoxy-2-tetralone

6-Methoxy-2-tetralone Structure
6-Methoxy-2-tetralone structure
CAS No.
2472-22-2
Chemical Name:
6-Methoxy-2-tetralone
Synonyms
6-methoxy-2-Tetrlone;4-dihydro-6-Methoxy-;6-METHOXY-2-TETRALONE;6-methoxyl-2-tetralone;6-Methoxytetralin-2-one;6-Methoxy-2-tetralone>6-METHOXY-2-TETRALONE 95%;6-Methoxy-2-tetralone,98%;6-Methoxy-2-tetralone,90%;6-Methoxy-2-tetralone,tech.90%
CBNumber:
CB4323880
Molecular Formula:
C11H12O2
Molecular Weight:
176.21
MDL Number:
MFCD00001729
MOL File:
2472-22-2.mol
MSDS File:
SDS
Last updated:2024-06-04 15:29:52
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6-Methoxy-2-tetralone Properties

Melting point 28-35 °C
Boiling point 114-116 °C (0.2 mmHg)
Density 1.0431 (rough estimate)
refractive index n20/D 1.5645(lit.)
Flash point >230 °F
storage temp. 2-8°C
form Crystalline Low Melting Solid
color Light yellow-beige to orange
Sensitive Air Sensitive
BRN 513418
InChI InChI=1S/C11H12O2/c1-13-11-5-3-8-6-10(12)4-2-9(8)7-11/h3,5,7H,2,4,6H2,1H3
InChIKey RMRKDYNVZWKAFP-UHFFFAOYSA-N
SMILES C1C2=C(C=C(OC)C=C2)CCC1=O
CAS DataBase Reference 2472-22-2(CAS DataBase Reference)
FDA UNII LAV9W5N9D9

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P233-P260-P261-P264-P271-P280-P302+P352-P304-P304+P340-P305+P351+P338-P312-P321-P332+P313-P337+P313-P340-P362-P403-P403+P233-P405-P501
Hazard Codes  Xi
Safety Statements  24/25
WGK Germany  3
HazardClass  IRRITANT
HS Code  29145090
NFPA 704
1
2 0

6-Methoxy-2-tetralone price More Price(22)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 184063 6-Methoxy-3,4-dihydro-2(1H)-naphthalenone 95% 2472-22-2 1g $66.2 2024-03-01 Buy
Sigma-Aldrich 184063 6-Methoxy-3,4-dihydro-2(1H)-naphthalenone 95% 2472-22-2 5g $314 2024-03-01 Buy
TCI Chemical M1317 6-Methoxy-2-tetralone >95.0%(GC) 2472-22-2 1g $81 2024-03-01 Buy
TCI Chemical M1317 6-Methoxy-2-tetralone >95.0%(GC) 2472-22-2 5g $395 2021-12-16 Buy
Alfa Aesar L11007 6-Methoxy-2-tetralone, tech. 90% 2472-22-2 1g $100 2021-12-16 Buy
Product number Packaging Price Buy
184063 1g $66.2 Buy
184063 5g $314 Buy
M1317 1g $81 Buy
M1317 5g $395 Buy
L11007 1g $100 Buy

6-Methoxy-2-tetralone Chemical Properties,Uses,Production

Description

6-methoxy-2-tetralone has been selected as the starting material for the synthesis of many steroidal compounds, including 2-aminotetalin derivatives, which exhibit antifungal activities, tetrahydro benzocycloheptane and many terpenoid compounds. 6-methoxy-2-tetralone is more expensive, difficult to synthesize, and unstable in comparison to 6-methoxy-1-tetralone[1].

Chemical Properties

light yellow-beige to orange

Uses

6-Methoxy-3,4-dihydro-2(1H)-naphthalenone was used in the synthesis of 1, 2, 3, 4-tetrahydro-2-naphthylamine derivatives.

Synthesis Reference(s)

Chemical and Pharmaceutical Bulletin, 9, p. 267, 1961 DOI: 10.1248/cpb.9.267
The Journal of Organic Chemistry, 26, p. 3237, 1961 DOI: 10.1021/jo01067a049

Synthesis

To a suspension of MCPBA (1.5g, 8.7mmol) in dry dichloromethane (16mL), cooled in ice, was added dihydro naphthalene (616mg, 3.8mmol) dissolved in dichloromethane (2mL). The reaction mixture was stirred overnight, filtered, diluted with dichloromethane, washed with a solution of sodium bicarbonate (5%), brine, dried, and evaporated to obtain an oil (591mg), which without purification was dissolved in ethanol (3mL) and treated with sulfuric acid (3mL, 10%) and heated under reflux for 3 hours. The reaction mixture was cooled, diluted with water, and extracted three times using chloroform. The organic extracts were washed with brine, dried, and evaporated to obtain an oil which, on purification (eluent hexane: ether 7:3), afforded 6-Methoxy-2-tetralone.

References

[1] Banerjee, A. K. et al. “A concise approach for the synthesis of 6-methoxy-2-tetralone.” 2018. 0.

6-Methoxy-2-tetralone synthesis

6099-04-3
2472-22-2
Synthesis of 6-Methoxy-2-tetralone from 3-Methoxycinnamic acid

6-Methoxy-2-tetralone Preparation Products And Raw materials

Raw materials

Preparation Products

6-Methoxy-2-tetralone Suppliers

Global( 194)Suppliers
Supplier Tel Email Country ProdList Advantage
PUSHAN INDUSTRIAL (SHAANXI) CO.,LTD
+8618291886785 olivia.wang@pushanshiye.com China 126 58
Hebei Mojin Biotechnology Co., Ltd 		+8613288715578 sales@hbmojin.com China 12470 58
Ouhuang Engineering Materials (Hubei) Co., Ltd 		+8617702722807 admin@hbouhuang.com China 3001 58
Hebei Zhuanglai Chemical Trading Co.,Ltd 		+8613343047651 admin@zlchemi.com China 2999 58
Capot Chemical Co.,Ltd. 		571-85586718 +8613336195806 sales@capotchem.com China 29797 60
Nanjing ChemLin Chemical Industry Co., Ltd. 		025-83697070 product@chemlin.com.cn CHINA 3012 60
career henan chemical co 		+86-0371-86658258 sales@coreychem.com China 29914 58
Hebei Guanlang Biotechnology Co., Ltd. 		+86-19930503282 alice@crovellbio.com China 8829 58
Chongqing Chemdad Co., Ltd 		+86-023-6139-8061 +86-86-13650506873 sales@chemdad.com China 39916 58
Wuhan Chemwish Technology Co., Ltd 		027-67849912 sales@chemwish.com CHINA 10828 58
Supplier Advantage
PUSHAN INDUSTRIAL (SHAANXI) CO.,LTD
58
Hebei Mojin Biotechnology Co., Ltd 		58
Ouhuang Engineering Materials (Hubei) Co., Ltd 		58
Hebei Zhuanglai Chemical Trading Co.,Ltd 		58
Capot Chemical Co.,Ltd. 		60
Nanjing ChemLin Chemical Industry Co., Ltd. 		60
career henan chemical co 		58
Hebei Guanlang Biotechnology Co., Ltd. 		58
Chongqing Chemdad Co., Ltd 		58
Wuhan Chemwish Technology Co., Ltd 		58

View Lastest Price from 6-Methoxy-2-tetralone manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
6-Methoxy-2-tetralone pictures 2024-06-06 6-Methoxy-2-tetralone
2472-22-2
 US $0.00 / kg 1kg 98% 2-5 MTs PUSHAN INDUSTRIAL (SHAANXI) CO.,LTD
6-Methoxy-2-tetralone pictures 2024-06-04 6-Methoxy-2-tetralone
2472-22-2
 US $10.00 / kg 1kg 99% 20ton Hebei Zhuanglai Chemical Trading Co.,Ltd
6-Methoxy-2-tetralone pictures 2024-04-22 6-Methoxy-2-tetralone
2472-22-2
 US $100.00-30.00 / kg 1kg 99.93% 1000kg per week Ouhuang Engineering Materials (Hubei) Co., Ltd

6-Methoxy-2-tetralone Spectrum

6-Methoxy-2-tetralone(2472-22-2)MS6-Methoxy-2-tetralone(2472-22-2)1HNMR6-Methoxy-2-tetralone(2472-22-2)13CNMR6-Methoxy-2-tetralone(2472-22-2)IR1

2472-22-2(6-Methoxy-2-tetralone )Related Search:

1,2,3,4-Tetrahydronaphthalene Decahydronaphthalene 1-Tetralone Nabumetone 6,7-Dimethoxy-2-tetralone
6,8-Dimethoxyl-2-tetralone 6,7-Dimethoxy-1-tetralone Methoxy-2-tetralone,5-,5-METHOXY-2-TETRALONE 6-Methoxy-1-Tetralone99% 8-METHOXY-2-TETRALONE
7-Methoxy-2-Tetralone(7-OHO),7-METHOXY-2-TETRALONE 7-METHOXY-1-TETRALONE,99.5+%,7-METHOXY-1-TETRALONE,7-Methoxy-1-tetralone/CH79635,7-Methoxy-1-tetralone,99% 6-methoxy-1-tetralone 8-Methoxy-α-Tetralone,8-METHOXY-A-TETRALONE,8-METHOXY-1-TETRALONE 5-METHOXY-1-TETRALONE,5-Methoxy-1-tetralone,97%,5-METHOXY-1-TETRALONE 97%,5-METHOXY-1-TETRALONE TECH 94+%
5-Chloro-8-methoxyl-2-tetralone 5,8-Dimethoxy-2-tetralone 6-METHOXY-1,2,3,4-TETRAHYDRONAPHTHALENE

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3,4-DIHYDRO-6-METHOXY-2(1H)-NAPHTHALENONE 6-methoxy-1,2,3,4-tetrahydronaphthalen-2-one 6-Methoxy-3,4-dihydro-2(1H)-naphthalenone, 95% 6-Methoxy-2-tetralone,tech.90% 6-methoxy-3,4-dihydro-1H-naphthalene-2-one 3,4-Dihydro-6-methoxynaphthalen-2(1H)-one 6-methoxy-2-Tetrlone 6-methoxy-3,4-dihydronaphthalen-2-one 6-METHOXY-2-TETRALONE: TECH., 90% 6-METHOXY-2-TETRALONE 95% 6-methoxyl-2-tetralone 6-Methoxytetralin-2-one 6-Methoxy-1,2,3,4-tetrahydronaphthalene-2-one 6-Methoxy-2-tetralone,98% 6-Methoxy-2-tetralone,90% 4-dihydro-6-Methoxy- 6-Methoxy-2-tetralone, 6-Methoxy-2-oxo-1,2,3,4-tetrahydronaphthalene 6-Methoxy-2-tetralone, technical, 90% 6-METHOXY-3,4-DIHYDRO-1H-NAPHTHALEN-2-ONE 6-METHOXY-2-TETRALONE 6-METHOXY-3,4-DIHYDRONAPHTHALEN-2(1H)-ONE 2(1H)-NAPHTHALENONE, 3,4-DIHYDRO-6-METHOXY- 6-Methoxy-2-tetralone> 2472-22-2 Organic Building Blocks Ketones Building Blocks C11 to C12 Carbonyl Compounds Fused Ring Systems pharmacetical Naphthalenes