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2,5-DIBROMOANISOLE

2,5-DIBROMOANISOLE Structure
2,5-DIBROMOANISOLE structure
CAS No.
95970-08-4
Chemical Name:
2,5-DIBROMOANISOLE
Synonyms
5-DIBROMOANISOLE;2,5-DIBROMOANISOL;2,5-DIBROMOANISOLE;1,4-dibroMo-2-Methoxybenzene;Benzene, 1,4-dibromo-2-methoxy-
CBNumber:
CB9138012
Molecular Formula:
C7H6Br2O
Molecular Weight:
265.93
MDL Number:
MFCD07780698
MOL File:
95970-08-4.mol
Last updated:2025-07-24 18:13:52
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2,5-DIBROMOANISOLE Properties

Boiling point 257-261 °C
Density 1.823±0.06 g/cm3(Predicted)
storage temp. Sealed in dry,Room Temperature
Appearance Light yellow to yellow Solid

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS06
Signal word  Danger
Hazard statements  H301
Precautionary statements  P264-P270-P301+P310-P321-P330-P405-P501

2,5-DIBROMOANISOLE price More Price(20)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TRC D422973 2,5-Dibromoanisole 95970-08-4 1g $55 2021-12-16 Buy
AK Scientific J53505 2,5-Dibromoanisole 95970-08-4 5g $72 2021-12-16 Buy
Biosynth Carbosynth FD142637 1,4-Dibromo-2-methoxybenzene 95970-08-4 1g $80 2021-12-16 Buy
AK Scientific J53505 2,5-Dibromoanisole 95970-08-4 1g $18 2021-12-16 Buy
AK Scientific J53505 2,5-Dibromoanisole 95970-08-4 10g $125 2021-12-16 Buy
Product number Packaging Price Buy
D422973 1g $55 Buy
J53505 5g $72 Buy
FD142637 1g $80 Buy
J53505 1g $18 Buy
J53505 10g $125 Buy

2,5-DIBROMOANISOLE Chemical Properties,Uses,Production

Chemical Properties

Off-white to yellow liquid crystalline

Uses

2,5-Dibromoanisole is mainly used in organic and pharmaceutical synthesis.

Synthesis

Methanol

67-56-1

1,4-DIBROMO-2-FLUOROBENZENE

1435-52-5

2,5-DIBROMOANISOLE

95970-08-4

The general procedure for the synthesis of 2,5-dibromo-1-methoxybenzene from methanol and 1,4-dibromo-2-fluorobenzene was as follows: to a mixture of 1,4-dibromo-2-fluorobenzene (25.0 g, 98.5 mmol) in a solution of tetrahydrofuran (492 mL) and methanol (40 mL, 984.7 mmol) was added slowly and dropwise potassium tert-butoxide (118.2 mL, 118.2 mmol, 1 M hexane solution). The reaction mixture was stirred at room temperature, then warmed to 70 °C and kept overnight. Upon completion of the reaction, the reaction was quenched with water (50 mL) and the reaction mixture was diluted with ether (400 mL) and subsequently washed once with saturated ammonium chloride solution (300 mL). The aqueous layer was back-extracted with ether (200 mL) and all organic phases were combined and dried over anhydrous sodium sulfate. After filtration, the organic phase was concentrated under reduced pressure to give the crude product. The crude product was purified by fast column chromatography using 5-10% ethyl acetate/hexane as eluent to give 22.0 g (84% yield) of 2,5-dibromo-1-methoxybenzene. The product was analyzed by gas chromatography and the m/z (79Br16Br) was 266 [M]+.

References

[1] Patent: WO2007/146758, 2007, A2. Location in patent: Page/Page column 76

2,5-DIBROMOANISOLE synthesis

19056-40-7
95970-08-4
Synthesis of 2,5-DIBROMOANISOLE from 4-BROMO-3-METHOXYANILINE

2,5-DIBROMOANISOLE Preparation Products And Raw materials

Raw materials

2-BROMO-5-NITROANISOLE 4-BROMO-3-METHOXYANILINE N-(2,5-dibromo-4-methoxyphenyl)acetamide 2,5-Dibromo-4-methoxyaniline 4-BROMO-2-METHOXYBENZOIC ACID
2,5-DIBROMOPHENOL 1,4-DIBROMO-2-FLUOROBENZENE Methanol Dimethyl sulfate Iodomethane
Methacetin 2-Methoxy-4-nitroaniline

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Preparation Products

2,4-DIBROMOANISOLE Benzenemethanol, α-ethenyl-2-hydroxy-

2,5-DIBROMOANISOLE Suppliers

Global( 113)Suppliers
Supplier Tel Email Country ProdList Advantage
Henan Fengda Chemical Co., Ltd 		+86-371-86557731 +86-13613820652 info@fdachem.com China 20202 58
Capot Chemical Co.,Ltd. 		+8613336195806 sales@capot.com China 29731 60
Zjartschem 		+86-571 87238903 jocelynpan@zjarts.com CHINA 988 58
SHANDONG ZHI SHANG CHEMICAL CO.LTD 		+86 18953170293 sales@sdzschem.com China 2930 58
Changzhou Ansciep Chemical Co., Ltd. 		+86 519 86305871 sales@ansciepchem.com CHINA 4241 58
Nanjing Dolon Biotechnology Co.,Ltd. 		18905173768 sales@dolonchem.com CHINA 2972 58
Alchem Pharmtech,Inc. 		8485655694 sales@alchempharmtech.com United States 63687 58
Shenzhen Excellent Biotech Co., Ltd. 		13480692018 ramyan@ex-biotech.com CHINA 954 58
career henan chemical co 		+86-0371-86658258 +8613203830695 factory@coreychem.com China 29804 58
Fuxin Pharmaceutical 		+86-021-021-50872116 +8613122107989 contact@fuxinpharm.com China 10035 58
Supplier Advantage
Henan Fengda Chemical Co., Ltd 		58
Capot Chemical Co.,Ltd. 		60
Zjartschem 		58
SHANDONG ZHI SHANG CHEMICAL CO.LTD 		58
Changzhou Ansciep Chemical Co., Ltd. 		58
Nanjing Dolon Biotechnology Co.,Ltd. 		58
Alchem Pharmtech,Inc. 		58
Shenzhen Excellent Biotech Co., Ltd. 		58
career henan chemical co 		58
Fuxin Pharmaceutical 		58

View Lastest Price from 2,5-DIBROMOANISOLE manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
2,5-Dibromoanisole pictures 2024-01-22 2,5-Dibromoanisole
95970-08-4
 US $8.00-0.80 / KG 1KG 99% g-kg-tons, free sample is available Henan Fengda Chemical Co., Ltd
1,4-dibromo-2-methoxybenzene pictures 2020-01-10 1,4-dibromo-2-methoxybenzene
95970-08-4
 US $1.00 / KG 1KG 98% HPLC 10 tons/month Career Henan Chemical Co

2,5-DIBROMOANISOLE Spectrum

2,5-DIBROMOANISOLE(95970-08-4)1HNMR

95970-08-4(2,5-DIBROMOANISOLE)Related Search:

PENTABROMOPHENYL METHACRYLATE 2,2',3,3',4,4',5,5',6-nonabromodiphenylether OCTABROMODIPHENYL ETHER 2,2',4,4',5,5'-HEXABROMODIPHENYL ETHER 1,4-Dibromo-2,5-dimethoxybenzene
TETRADECABROMO-1,4-DIPHENOXYBENZENE Pentabromodiphenyl ether 2,2',4,4',5,6'-HEXABROMODIPHENYL ETHER PENTABROMOPHENYL ACRYLATE Decabromodiphenyl oxide
2,2',4,4',5-PENTABROMODIPHENYL ETHER 2,5-DIBROMOANISOLE 2,5-DIBROMO(TRIFLUOROMETHOXY)BENZENE 2,2',3,4,4',5,5',6'-OCTABROMODIPHENYL ETHER 2,5-DIBROMO-4-(DECYLOXY)PHENOL, 99%
1,4-DIBROMO-2,5-BIS(3-SULFONATOPROPOXY)BENZENE DISODIUM SALT 1,2,3,4-TETRABROMO-5,6-DIMETHOXYBENZENE 1,4-DIBROMO-2,5-BIS(DECYLOXY)BENZENE

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2,5-DIBROMOANISOLE 1,4-dibroMo-2-Methoxybenzene 2,5-DIBROMOANISOL Benzene, 1,4-dibromo-2-methoxy- 5-DIBROMOANISOLE 95970-08-4 Anisoles, Alkyloxy Compounds & Phenylacetates Bromine Compounds