7-니트로-1,2,3,4-테트라히드로퀴놀린

7-니트로-1,2,3,4-테트라히드로퀴놀린
7-니트로-1,2,3,4-테트라히드로퀴놀린 구조식 이미지
카스 번호:
30450-62-5
한글명:
7-니트로-1,2,3,4-테트라히드로퀴놀린
동의어(한글):
7-니트로-1,2,3,4-테트라히드로퀴놀린
상품명:
7-Nitro-1,2,3,4-tetrahydroquinoline
동의어(영문):
7-Nitro-1;7-Nitro-1,2,3,4-Terahydroquinoline;7-NITRO-1,2,3,4-TETRAHYDROQUINOLINE;1,2,3,4-TETRAHYDRO-7-NITROQUINOLINE;7-Nitro-1,2,3,4-tetrahydroquinoline>Quinoline, 1,2,3,4-tetrahydro-7-nitro-;7-Nitro-1,2,3,4-tetrahydroquinoline,95%;7-NITRO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE;7-Nitro-1,2,3,4-tetrahydroquinoline 1,2,3,4-Tetrahydro-7-nitroquinoline
CBNumber:
CB6246251
분자식:
C9H10N2O2
포뮬러 무게:
178.19
MOL 파일:
30450-62-5.mol

7-니트로-1,2,3,4-테트라히드로퀴놀린 속성

녹는점
61.0 to 65.0 °C
끓는 점
325.2±31.0 °C(Predicted)
밀도
1.236±0.06 g/cm3(Predicted)
저장 조건
Keep in dark place,Sealed in dry,Room Temperature
용해도
메탄올에 용해됨
산도 계수 (pKa)
3.44±0.20(Predicted)
물리적 상태
가루
색상
빨간색
CAS 데이터베이스
30450-62-5(CAS DataBase Reference)
안전
  • 위험 및 안전 성명
  • 위험 및 사전주의 사항 (GHS)
위험품 표기 T
위험 카페고리 넘버 25
안전지침서 45
유엔번호(UN No.) UN 2811 6.1 / PGIII
HS 번호 2933499090
그림문자(GHS): GHS hazard pictograms
신호 어: Danger
유해·위험 문구:
암호 유해·위험 문구 위험 등급 범주 신호 어 그림 문자 P- 코드
H301 삼키면 유독함 급성 독성 물질 - 경구 구분 3 위험 GHS hazard pictograms P264, P270, P301+P310, P321, P330,P405, P501
예방조치문구:
P301+P310 삼켰다면 즉시 의료기관(의사)의 진찰을 받으시오.
NFPA 704
1
2 0

7-니트로-1,2,3,4-테트라히드로퀴놀린 C화학적 특성, 용도, 생산

Synthesis

7-Nitro-1,2,3,4-tetrahydroquinoline is synthesised by the reaction of 1,2,3,4-tetrahydroquinoline and nitric acid in sulphuric acid solution. The specific synthesis steps are as follows:
Concentrated sulfuric acid (30.00 mL) was cooled to -10° C. with an ice/salt bath. To this, 1,2,3,4-tetrahydro-quinoline (10.60 g, 75.60 mmol) and a solution of nitric acid (99.5percent, 4.80 g, 75.60 mmol) in sulfuric acid (15.00 mL) were added simultaneously within 1 hour, so that the temperature of the reaction mixture does not exceed 10° C. The mixture was stirred then for 2.5 hours at -5° C., then poured over ice and treated with sodium carbonate (0.10 kg) until pH 8-9 was reached. The solid was filtered, washing with water, then dissolved in dichloromethane. The organic phase was washed with water, dried over magnesium sulphate and evaporated. 7-Nitro-1,2,3,4-tetrahydro-quinoline was obtained as a viscous brown oil, 13.70 g (85percent), 84percent purity.
7-Nitro-1,2,3,4-tetrahydroquinoline synthesis

7-니트로-1,2,3,4-테트라히드로퀴놀린 준비 용품 및 원자재

원자재

준비 용품


7-니트로-1,2,3,4-테트라히드로퀴놀린 공급 업체

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Springchem New Material Technology Co.,Limited
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Alchem Pharmtech,Inc.
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career henan chemical co
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SIMAGCHEM CORP
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Hefei TNJ Chemical Industry Co.,Ltd.
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sales@tnjchem.com China 34571 58
Jinjiangchem Corporation
512-50133713
sales@jinjiangchem.com CHINA 1072 58

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