1,3-dibromo-5-(tert-butyl)-2-methoxybenzene synthesis
- Product Name:1,3-dibromo-5-(tert-butyl)-2-methoxybenzene
- CAS Number:132268-08-7
- Molecular formula:C11H14Br2O
- Molecular Weight:322.04
Yield:132268-08-7 92%
Reaction Conditions:
Stage #1: 2,6-dibromo-4-tert-butylphenolwith sodium hydride in tetrahydrofuran at 0; for 0.333333 h;Inert atmosphere;Schlenk technique;Glovebox;
Stage #2: dimethyl sulfate in tetrahydrofuran at 0 - 55; for 12.5 h;Inert atmosphere;Schlenk technique;Glovebox;
References:
Koch, Felix;Schubert, Hartmut;Sirsch, Peter;Berkefeld, Andreas [Dalton Transactions,2015,vol. 44,# 29,p. 13315 - 13324] Location in patent:supporting information
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