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ChemicalBook CAS DataBase List 1,4-Diaminobutane dihydrochloride
333-93-7

1,4-Diaminobutane dihydrochloride synthesis

6synthesis methods
-

Yield:333-93-7 95%

Reaction Conditions:

Stage #1: butanedinitrilewith cobalt pivalate;1,1,3,3-Tetramethyldisiloxane;tert-butylisonitrile at 80; for 24 h;
Stage #2: with hydrogenchloride in diethyl ether at 20; for 0.5 h;

References:

Sanagawa, Atsushi;Nagashima, Hideo [Organic Letters,2019,vol. 21,# 1,p. 287 - 291] Location in patent:supporting information

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