1,6-dimethylpyridine: sulfooxymethane synthesis
1synthesis methods
- Product Name:1,6-dimethylpyridine: sulfooxymethane
- CAS Number:2037-39-0
- Molecular formula:C8H15NO4S
- Molecular Weight:221.274
Yield:-
Reaction Conditions:
in ethanol at 59.84; for 4 h;
Steps:
7.a
Example 7Preparation of the Compound of Formula (107) (a) Alkylation2-methyl-pyridine (68.8 g) are dissolved in 80 ml absolute ethanol.The temperature is raised to 333 K.94 g dimethylsulfate are introduced in this mixture within one hour.The temperature is maintained at 333 K during the following 3 h.
References:
US2009/113639,2009,A1 Location in patent:Page/Page column 25