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22248-13-1

1-(6-Hydroxy-2,3-dimethoxyphenyl)ethanone synthesis

3synthesis methods
Preparation by reaction of dimethyl sulfate on 3,6- di-hydroxy-2-methoxyacetophenone with potassium carbonate in boiling benzene (67%).
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Yield:22248-13-1 620 mg

Reaction Conditions:

with potassium carbonate in acetone;

References:

Wollenweber, Eckhard;Iinuma, Munekazu;Tanaka, Toshiyuki;Mizuno, Mizuo [Phytochemistry,1990,vol. 29,# 2,p. 633 - 637]