1-methyl-1H-pyrrolo[2,3-c]pyridine synthesis
- Product Name:1-methyl-1H-pyrrolo[2,3-c]pyridine
- CAS Number:860297-49-0
- Molecular formula:C8H8N2
- Molecular Weight:132.16
271-29-4
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77-78-1
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Yield:860297-49-0 77%
Reaction Conditions:
Stage #1: 1H-pyrrolo[2,3-c]pyridinewith sodium hydride in N,N-dimethyl-formamide;mineral oil;Inert atmosphere;
Stage #2: dimethyl sulfuric acid in N,N-dimethyl-formamide;mineral oil at 0 - 20; for 19 h;Inert atmosphere;
References:
Huestis, Malcolm P.;Fagnou, Keith [Organic Letters,2009,vol. 11,# 6,p. 1357 - 1360] Location in patent:supporting information; experimental part
271-29-4
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74-88-4
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21898-65-7
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1003-29-8
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1192-58-1
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