Cyclohexanecarboxylic acid, 1-methyl-4-oxo-, ethyl ester synthesis
- Product Name:Cyclohexanecarboxylic acid, 1-methyl-4-oxo-, ethyl ester
- CAS Number:147905-77-9
- Molecular formula:C10H16O3
- Molecular Weight:184.23
![ethyl 1,4-dioxaspiro[4.5]decane-8-carboxylate](/CAS/GIF/1489-97-0.gif)
1489-97-0
137 suppliers
$17.00/1g
147905-77-9
80 suppliers
$41.00/100mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1.) i-Pr2NLi / 1.) pentane, THF, HMPA, -70 deg C, 20 min, 2.) pentane, THF, HMPA, -70 deg C to r.t.
2: 91 percent / 1M H2SO4 / acetone / 24 h / Ambient temperature
References:
Della;Knill [Australian Journal of Chemistry,1994,vol. 47,# 10,p. 1833 - 1841]
![Ethyl 8-Methyl-1,4-dioxa-spiro[4,5]decane-8-carboxylate](/CAS/20150408/GIF/24730-88-9.gif)
24730-88-9
56 suppliers
$18.00/100mg
147905-77-9
80 suppliers
$41.00/100mg
144-55-8
1294 suppliers
$10.00/25g
24730-88-9
56 suppliers
$18.00/100mg
147905-77-9
80 suppliers
$41.00/100mg
860469-35-8
18 suppliers
$698.00/5g
77-78-1
287 suppliers
$19.69/1ml
147905-77-9
80 suppliers
$41.00/100mg
17159-79-4
331 suppliers
$5.00/1g
147905-77-9
80 suppliers
$41.00/100mg