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ChemicalBook CAS DataBase List 2,5-DIMETHOXYBENZENETHIOL
2570-42-5

2,5-DIMETHOXYBENZENETHIOL synthesis

7synthesis methods
-

Yield:2570-42-5 99%

Reaction Conditions:

Stage #1: 2,5-dimethoxythiophenolwith potassium hydroxide in methanol; for 1 h;
Stage #2: dimethyl sulfate in methanol; for 0.5 h;Heating;

References:

Gallardo-Godoy, Alejandra;Fierro, Angélica;McLean, Thomas H.;Castillo, Mariano;Cassels, Bruce K.;Reyes-Parada, Miguel;Nichols, David E. [Journal of Medicinal Chemistry,2005,vol. 48,# 7,p. 2407 - 2419]