2-Ethylhexyl acetate synthesis
- Product Name:2-Ethylhexyl acetate
- CAS Number:103-09-3
- Molecular formula:C10H20O2
- Molecular Weight:172.26
104-76-7
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$5.00/10g
79-20-9
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$14.00/100g
67-56-1
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$7.29/5ml-f
103-09-3
282 suppliers
$6.00/25g
Yield:103-09-3 90.9%
Reaction Conditions:
with NKC-9 at 80; for 3 h;Catalytic behavior;Reagent/catalyst;Temperature;
Steps:
Transesterification reaction procedure: All the experiments were conducted in a 4-neck round bottom flask of volume250 mL equipped with a stirrer, a thermometer, a condenserpipe and a pressure-equalizing dropping funnel. The 4-neckround bottom flask was dipped in a constant temperature waterbath which was equipped with a temperature sensor. 2-Ethylhexanol and NKC-9 were put into the 4-neck round bottomflask. The temperature in the reactor was maintained within±1 °C with respect to the desired temperature. The measuredquantities of 2-ethylhexanol and NKC-9 were charged intothe 4-neck round bottom flask and methyl acetate was chargedto the constant pressure drop funnel. Once the desired temperature was achieved, the methyl acetate was being droppedinto the reactive mixture over a 2 h period. After the droppingwas finished, the temperature is maintained at the desiredtemperature for the fixed time. NKC-9 and the reactive liquidwere separated by vacuum filtration when it cooled down andthe NKC-9 was recycled at the same time. Finally the fractionbetween 130 and 140 °C was collected by reduced pressuredistillation and weighed this fraction.
References:
Yin, Lina;Wang, Dazhi;Qu, Fengzuo;Jia, Lin;Zhang, Shaoyin [Asian Journal of Chemistry,2015,vol. 27,# 8,p. 2861 - 2864]
104-76-7
648 suppliers
$5.00/10g
79-20-9
522 suppliers
$14.00/100g
123-11-5
821 suppliers
$10.00/10g
103-09-3
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$6.00/25g
5466-77-3
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$24.00/1g
1653-40-3
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$165.00/250mg
79-20-9
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$14.00/100g
103-09-3
282 suppliers
$6.00/25g
108-05-4
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$4.00/1000g
104-76-7
648 suppliers
$5.00/10g
103-09-3
282 suppliers
$6.00/25g