2-Methyl-3-(3,4-methylenedioxyphenyl)propanal synthesis
- Product Name:2-Methyl-3-(3,4-methylenedioxyphenyl)propanal
- CAS Number:1205-17-0
- Molecular formula:C11H12O3
- Molecular Weight:192.21
6974-47-6
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1205-17-0
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Yield:1205-17-0 14 g
Reaction Conditions:
with hydrogen in ethanol at 30; for 7 h;Autoclave;Temperature;Reagent/catalyst;
Steps:
2
15 g of the above-prepared piperonylidenpropanal was dissolved in 50 ml of ethanol,Into a high pressure reactor.Then add 1.5 ~ 1.8gP-2-Ni-Cu with hydrogen replacement reactor in the air,The hydrogen pressure in the autoclave was raised to 3 Kg · (cm2) -1,Temperature 30 reaction 7h.The reaction was terminated to room temperature,Reduced to atmospheric pressure,The reaction was filtered,The filtrate was distilled under pressure, and 134-135 ° C (399Pa) -1 was collected to obtain 14 g of helional.
References:
CN103880812,2016,B Location in patent:Page/Page column 4; 5
94-59-7
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201230-82-2
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52417-30-8
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1205-17-0
336 suppliers
$7.00/5g
94-59-7
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$32.00/10mg
201230-82-2
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52417-30-8
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1205-17-0
336 suppliers
$7.00/5g
17627-76-8
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![5-[(E)-prop-1-enyl]benzo[1,3]dioxole](/CAS/GIF/4043-71-4.gif)
4043-71-4
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