3,3',4,4'-TETRACHLOROAZOBENZENE synthesis
- Product Name:3,3',4,4'-TETRACHLOROAZOBENZENE
- CAS Number:14047-09-7
- Molecular formula:C12H6Cl4N2
- Molecular Weight:320
95-76-1
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Yield: 89%
Reaction Conditions:
with sodium perborate;Dihydrate sodium molybdate in acetic acid at 50; for 1 h;Kinetics;Thermodynamic data;Catalytic behavior;Temperature;
Steps:
General procedure: SPB (0.011 mol) and Na2MoO4 (0.001 mol) were dissolved in glacial acetic acid (5-7 mL) and aniline (0.015 mol) was added drop-wise or in portions at 50 °C.The temperature was maintained at 50 °C for an hour. The resultant was poured into water (500 mL) and stirred. The solid was filtered, dried and recrystallized from petroleum ether (40-60 °C).
References:
Karunakaran;Venkataramanan [Chemical Papers,2019,vol. 73,# 2,p. 375 - 385]
99-54-7
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102-71-6
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619-08-9
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95-76-1
376 suppliers
$10.00/5g
14047-09-7
17 suppliers
inquiry