3-BroMo-9-(4-broMophenyl)carbazole synthesis
- Product Name:3-BroMo-9-(4-broMophenyl)carbazole
- CAS Number:1226860-66-7
- Molecular formula:C18H11Br2N
- Molecular Weight:401.09
1592-95-6
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$5.00/1g
460-00-4
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$6.00/10g
1226860-66-7
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$32.00/100mg
Yield: 73%
Reaction Conditions:
with caesium carbonate in N,N-dimethyl-formamide at 150; for 24 h;
Steps:
Metal-Free N-Arylation of Carbazoles; General Procedure
General procedure: A mixture of a fluorinated aryl halide (2.0 mmol), a carbazole (0.5 mmol), and a base (2.0 mmol) in solvent (2 mL) was allowed to react under air atmosphere. The reaction mixture was heated to the specified temperature for 24 h. After reaction completion, the mixture was added to brine (15 mL) and extracted with CH2Cl2 (3 × 15 mL). The combined extract was concentrated under reduced pressure and the product was isolated by short chromatography on a silica gel (200-300 mesh) column.
References:
Wang, Lei;Ji, Enhui;Liu, Ning;Dai, Bin [Synthesis,2016,vol. 48,# 5,p. 737 - 750]
57102-42-8
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1226860-66-7
61 suppliers
$32.00/100mg
1592-95-6
408 suppliers
$5.00/1g
589-87-7
540 suppliers
$10.00/1g
1226860-66-7
61 suppliers
$32.00/100mg
589-87-7
540 suppliers
$10.00/1g
1226860-66-7
61 suppliers
$32.00/100mg
86-74-8
341 suppliers
$10.00/5g
1226860-66-7
61 suppliers
$32.00/100mg