3-methoxybut-1-ene synthesis
- Product Name:3-methoxybut-1-ene
- CAS Number:17351-24-5
- Molecular formula:C5H10O
- Molecular Weight:86.13
Yield:-
Reaction Conditions:
with rhodium(III) chloride;silica gel in m-xylene at 100; under 3800.26 Torr; for 1 h;
Steps:
1 Example 1
In a 450 ml high-pressure reactor, 23.5 g of 1,3-butadiene (BD) and 27.8 g of solvent and methanol were added to 270 ml of meta-xylene as a solvent, and in the presence of a catalyst (RhCl3/SiO2), while stirring at a pressure of 5 atm and 100° C. for 1 hour Reacted. The 3-methoxy-1-butene generated after the reaction was recovered through a distillation process.
References:
KR2020/62420,2020,A Location in patent:Paragraph 0035-0036
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