ChemicalBook CAS DataBase List 3-METHYLPENTANE-1,3,5-TRIOL

3-METHYLPENTANE-1,3,5-TRIOL synthesis

12synthesis methods

Product Name:3-METHYLPENTANE-1,3,5-TRIOL
CAS Number:7564-64-9
Molecular formula:C6H14O3
Molecular Weight:134.17

105-50-0 Synthesis

105-50-0
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Yield:-

Steps:

Multi-step reaction with 6 steps
1: 92 percent / BF₃*Et₂O / CH₂Cl₂ / 6 h / Ambient temperature
2: 90 percent / LiAlH₄ / tetrahydrofuran / 1 h / Heating
3: 100 percent / p-toluenesulphonic acid / CH₂Cl₂ / 4 h / 0 °C
4: 96 percent / CaCO₃, HgCl₂ / acetonitrile; H₂O / 1 h / Ambient temperature
5: 1) Mg / 1) ether, 2) 0 deg C, 15 min
6: 90 percent / p-toluenesulphonic acid / methanol / 4 h / Heating

References:

Chakraborty, T. K.;Bhushan, Vidya;Chandrasekaran, S. [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1983,vol. 22,# 1,p. 9 - 11]

674-26-0 Synthesis