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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

4(3H)-Quinazolinone,3-(chloromethyl)-(6CI) synthesis

4synthesis methods
491-36-1 Synthesis
4-Hydroxyquinazoline

491-36-1
324 suppliers
$5.00/25mg

50-00-0 Synthesis
Formaldehyde

50-00-0
839 suppliers
$10.00/25g

4(3H)-Quinazolinone,3-(chloromethyl)-(6CI)

99067-49-9
9 suppliers
inquiry

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Yield:99067-49-9 89%

Reaction Conditions:

Stage #1: 4-Hydroxyquinazoline;formaldehyd in water;Heating;
Stage #2: with thionyl chloride in dichloromethane;N,N-dimethyl-formamide at 20;Further stages.;

References:

Cho, Su-Dong;Hwang, Jaeyoung;Kim, Ho-Kyun;Yim, Heung-Sup;Kim, Jeum-Jong;Lee, Sang-Gyeong;Yoon, Yong-Jin [Journal of Heterocyclic Chemistry,2007,vol. 44,# 4,p. 951 - 960]

491-36-1 Synthesis
4-Hydroxyquinazoline

491-36-1
324 suppliers
$5.00/25mg

4(3H)-Quinazolinone,3-(chloromethyl)-(6CI)

99067-49-9
9 suppliers
inquiry

References
3-(Hydroxymethyl)quinazolin-4(3H)-one

14663-52-6
5 suppliers
inquiry

4(3H)-Quinazolinone,3-(chloromethyl)-(6CI)

99067-49-9
9 suppliers
inquiry

References
Anthranilic acid

118-92-3
4 suppliers
$23.00/250g

4(3H)-Quinazolinone,3-(chloromethyl)-(6CI)

99067-49-9
9 suppliers
inquiry

References