4-(BENZYLTHIO)PHENOL synthesis
- Product Name:4-(BENZYLTHIO)PHENOL
- CAS Number:30519-03-0
- Molecular formula:C13H12OS
- Molecular Weight:216.3
637-89-8
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$24.00/5g
100-44-7
659 suppliers
$13.50/250G
30519-03-0
13 suppliers
$110.00/50mg
Yield:30519-03-0 96%
Reaction Conditions:
with triethylamine in chloroform; for 8 h;Reflux;
Steps:
1.1 Preparation of 1,4- (Benzylthio) phenol:
12.6 g (0.1 mol) of 4-mercaptophenol and 12.12 g (0.12 mol) of triethylamine were added to a three-necked reaction flask equipped with a thermometer and an electric stirrer, and 12.6 (0.1 mol) of benzyl chloride 100ml of chloroform solution, dropping time is 2h. Then heated to reflux for 6 h. After completion of the reaction, poured into 150ml of water, the separation of several layers, washed with 3 × 100ml of water, anhydrous sodium sulfate and concentrated to a yellow solid 4- (benzylthio) phenol, and then recrystallization from anhydrous methanol, yellow Solid 20.7 g Yield 96%
References:
CN105541686,2016,A Location in patent:Paragraph 0023; 0026; 0027; 0028
637-89-8
179 suppliers
$24.00/5g
100-39-0
437 suppliers
$10.00/10g
30519-03-0
13 suppliers
$110.00/50mg
123-30-8
625 suppliers
$10.00/5g
100-44-7
659 suppliers
$13.50/250G
30519-03-0
13 suppliers
$110.00/50mg
106-41-2
501 suppliers
$13.00/5g
100-39-0
437 suppliers
$10.00/10g
30519-03-0
13 suppliers
$110.00/50mg
533-58-4
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$6.00/5g
100-53-8
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$10.00/1g
30519-03-0
13 suppliers
$110.00/50mg