![](/CAS/GIF/30519-03-0.gif)
4-(BENZYLTHIO)PHENOL synthesis
- Product Name:4-(BENZYLTHIO)PHENOL
- CAS Number:30519-03-0
- Molecular formula:C13H12OS
- Molecular Weight:216.3
![4-Mercaptophenol](/CAS/GIF/637-89-8.gif)
637-89-8
166 suppliers
$24.00/5g
![Benzyl chloride](/CAS/GIF/100-44-7.gif)
100-44-7
628 suppliers
$13.50/250G
![4-(BENZYLTHIO)PHENOL](/CAS/GIF/30519-03-0.gif)
30519-03-0
12 suppliers
$110.00/50mg
Yield:30519-03-0 96%
Reaction Conditions:
with triethylamine in chloroform; for 8 h;Reflux;
Steps:
1.1 Preparation of 1,4- (Benzylthio) phenol:
12.6 g (0.1 mol) of 4-mercaptophenol and 12.12 g (0.12 mol) of triethylamine were added to a three-necked reaction flask equipped with a thermometer and an electric stirrer, and 12.6 (0.1 mol) of benzyl chloride 100ml of chloroform solution, dropping time is 2h. Then heated to reflux for 6 h. After completion of the reaction, poured into 150ml of water, the separation of several layers, washed with 3 × 100ml of water, anhydrous sodium sulfate and concentrated to a yellow solid 4- (benzylthio) phenol, and then recrystallization from anhydrous methanol, yellow Solid 20.7 g Yield 96%
References:
CN105541686,2016,A Location in patent:Paragraph 0023; 0026; 0027; 0028
![4-Mercaptophenol](/CAS/GIF/637-89-8.gif)
637-89-8
166 suppliers
$24.00/5g
![Benzyl bromide](/CAS/GIF/100-39-0.gif)
100-39-0
424 suppliers
$10.00/10g
![4-(BENZYLTHIO)PHENOL](/CAS/GIF/30519-03-0.gif)
30519-03-0
12 suppliers
$110.00/50mg
![4-Aminophenol](/CAS/GIF/123-30-8.gif)
123-30-8
605 suppliers
$10.00/5g
![Benzyl chloride](/CAS/GIF/100-44-7.gif)
100-44-7
628 suppliers
$13.50/250G
![4-(BENZYLTHIO)PHENOL](/CAS/GIF/30519-03-0.gif)
30519-03-0
12 suppliers
$110.00/50mg
![4-Bromophenol](/CAS/GIF/106-41-2.gif)
106-41-2
483 suppliers
$13.00/5g
![Benzyl bromide](/CAS/GIF/100-39-0.gif)
100-39-0
424 suppliers
$10.00/10g
![4-(BENZYLTHIO)PHENOL](/CAS/GIF/30519-03-0.gif)
30519-03-0
12 suppliers
$110.00/50mg
![2-Iodophenol](/CAS/GIF/533-58-4.gif)
533-58-4
361 suppliers
$6.00/5g
![Benzyl mercaptan](/CAS/GIF/100-53-8.gif)
100-53-8
235 suppliers
$10.00/1g
![4-(BENZYLTHIO)PHENOL](/CAS/GIF/30519-03-0.gif)
30519-03-0
12 suppliers
$110.00/50mg