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3393-00-8

4-bromo-4'-methylsulfanyl-biphenyl synthesis

8synthesis methods
106-37-6 Synthesis
1,4-Dibromobenzene

106-37-6
487 suppliers
$9.00/5g

98546-51-1 Synthesis
4-(Methylthio)phenylboronic acid

98546-51-1
273 suppliers
$5.00/1g

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Yield:3393-00-8 96.4%

Reaction Conditions:

with tetrakis(triphenylphosphine) palladium(0);sodium carbonate in ethanol;water;toluene; for 24 h;Inert atmosphere;Reflux;

References:

Ding, Siyang;Huang, Miaoling;Li, Jinshi;Qian, Jingyu;Shen, Pingchuan;Tang, Ben Zhong;Xu, Bin;Zhao, Zujin;Zhou, Xiao-Shun [Angewandte Chemie - International Edition,2020,vol. 59,# 11,p. 4581 - 4588][Angew. Chem.,2020,vol. 132,p. 4611 - 4618,8] Location in patent:supporting information