(4-Methylpiperazin-1-yl)(4-nitrophenyl)Methanone synthesis

5synthesis methods

50-00-0 Synthesis

72141-41-4 Synthesis

Yield:21091-98-5 900 mg

Reaction Conditions:

with sodium tris(acetoxy)borohydride;triethylamine in dichloromethane at 20; for 3 h;

Steps:

1.1

Step 1’: 1 g of 1’ was converted to 2’ using CH₂O/NaBH(OAc)3/TEA/DCM/RT/3h. After purification, 900 mg of 2’ was obtained.

References:

WO2021/236650,2021,A1 Location in patent:Page/Page column 172; 219

109-01-3 Synthesis

109-01-3 Synthesis

62-23-7 Synthesis

367-24-8 Synthesis

109-01-3 Synthesis

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