7,8-dihydropyrano[4,3-b]pyridin-5-one synthesis
- Product Name:7,8-dihydropyrano[4,3-b]pyridin-5-one
- CAS Number:5860-72-0
- Molecular formula:C8H7NO2
- Molecular Weight:149.15
2942-59-8
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 84 percent / K2CO3 / acetone / 25 °C
2: 70 percent / 2,6-di-t-butyl-4-methylphenol / (Ph3P)2Pd(II)Cl2 / dimethylformamide / 68 h / 40 - 55 °C
3: 14 percent / NH4Cl / acetic acid; H2O / 5 h / Heating
References:
Showalter, H. D. Hollis [Journal of Heterocyclic Chemistry,2006,vol. 43,# 5,p. 1311 - 1317]
40134-18-7
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1721-26-2
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50-00-0
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1000210-73-0
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