7-NITRO-QUINOLINE synthesis
- Product Name:7-NITRO-QUINOLINE
- CAS Number:613-51-4
- Molecular formula:C9H6N2O2
- Molecular Weight:174.16
3054-95-3
208 suppliers
$28.00/25g
99-09-2
20 suppliers
$14.00/1g
613-51-4
126 suppliers
$8.00/250mg
Yield: 25.8 %Chromat.
Reaction Conditions:
with Ni-modified Beta zeolite in neat (no solvent) for 0.0833333 h;Microwave irradiation;Reflux;Green chemistry;
Steps:
2.2. Catalytic performance evaluation
General procedure: General procedure for synthesis of quinolines from anilines and ADA was carried out in Panasonic NN-K5541JF microwave oven reactor equipping a magnetic stirring device. The typical procedures were as follows: ADA (1mmol), excessive anilines (4mmol) and solid catalyst were charged into a round-bottom ask; and then, the mixtures was placed into microwave reactor. The reaction was conducted by continuous microwave irradiation for 1-40 min under refluxing and stirring condition. Finally, the resulting products were determined by GC-MS of Varian Saturn 2200/ CP-3800 gas chromatography-mass spectrometry equipped with two CP8944 capillary columns (VF-5,30m×0.25mm×0.25 μm).
References:
Li, An;Yang, Zan;Yang, Tao;Luo, Cai-Wu;Chao, Zi-Sheng;Zhou, Cong-Shan [Catalysis Communications,2018,vol. 115,p. 21 - 25]
30450-62-5
171 suppliers
$8.00/5g
613-51-4
126 suppliers
$8.00/250mg
56-81-5
1700 suppliers
$5.00/25g
99-09-2
20 suppliers
$14.00/1g
607-34-1
234 suppliers
$14.00/1g
613-51-4
126 suppliers
$8.00/250mg
30450-62-5
171 suppliers
$8.00/5g
98-95-3
27 suppliers
$14.00/25g
613-51-4
126 suppliers
$8.00/250mg
62-53-3
679 suppliers
$10.00/1g
91-22-5
407 suppliers
$10.00/25g
607-34-1
234 suppliers
$14.00/1g
613-51-4
126 suppliers
$8.00/250mg