Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List N-benzyl-2-(3,4-diMethoxyphenyl)-N-MethylethanaMine
96025-46-6

N-benzyl-2-(3,4-diMethoxyphenyl)-N-MethylethanaMine synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 2.) NaBH4 / 1.) 120 deg C, 2.5 h, 2.) CHCl3, EtOH, r.t., 8 h
2: 1.) H3BO3, 2.) NaBH4 / 1.) CH3OH, H2O, r.t.
3: 16.4 percent / KI / Ni(PPh3)2Cl2-Zn-PPh3 / dimethylformamide / 55 °C

References:

Kihara, Masaru;Itoh, Joji;Iguchi, Seiichiro;Imakura, Yasuhiro;Kobayashi, Shigeru [Journal of Chemical Research, Miniprint,1988,# 1,p. 157 - 177]