N-benzyl-2-(3,4-diMethoxyphenyl)-N-MethylethanaMine synthesis
- Product Name:N-benzyl-2-(3,4-diMethoxyphenyl)-N-MethylethanaMine
- CAS Number:96025-46-6
- Molecular formula:C18H23NO2
- Molecular Weight:285.38
63375-81-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 2.) NaBH4 / 1.) 120 deg C, 2.5 h, 2.) CHCl3, EtOH, r.t., 8 h
2: 1.) H3BO3, 2.) NaBH4 / 1.) CH3OH, H2O, r.t.
3: 16.4 percent / KI / Ni(PPh3)2Cl2-Zn-PPh3 / dimethylformamide / 55 °C
References:
Kihara, Masaru;Itoh, Joji;Iguchi, Seiichiro;Imakura, Yasuhiro;Kobayashi, Shigeru [Journal of Chemical Research, Miniprint,1988,# 1,p. 157 - 177]
120-20-7
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