ChemicalBook CAS DataBase List Acetic acid hydroxyammonium salt

Acetic acid hydroxyammonium salt synthesis

4synthesis methods

Product Name:Acetic acid hydroxyammonium salt
CAS Number:22606-42-4
Molecular formula:C2H7NO3
Molecular Weight:93.08188

127-09-3 Synthesis

127-09-3
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22606-42-4
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Yield:22606-42-4 98%

Reaction Conditions:

with hydroxylamine hydrochloride in water

Steps:

3.2.2. Hydroxylamine Acetate
Hydroxylamine hydrochloride (10.0 g, 144 mmol) was dissolved in deionized water (5 mL).The solution was added, on stirring, to a solution of sodium acetate (11.8 g, 144 mmol) in water(5 mL). The resulting clear solution was concentrated to dryness. The solid residue was suspended inanhydrous methanol (20 mL) and filtered to remove sodium chloride. The filtrate was concentrated invacuo to give hydroxylamine acetate (13.0 g, 141 mmol, 98%). 1H-NMR (400 MHz, DMSO-d6) 8.20(s, 4H, NH2OH, COOH), 1.86 (s, 3H, CH3) [27].

References:

Chupakhin, Evgeny;Bakulina, Olga;Dar’in, Dmitry;Krasavin, Mikhail [Molecules,2019,vol. 24,# 5,art. no. 864]

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64-19-7 Synthesis