Cyclopropyl 4-methoxyphenyl ketone synthesis
- Product Name:Cyclopropyl 4-methoxyphenyl ketone
- CAS Number:7152-03-6
- Molecular formula:C11H12O2
- Molecular Weight:176.21
4023-34-1
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$12.00/5g
100-66-3
541 suppliers
$10.00/5G
7152-03-6
94 suppliers
$15.00/5 g
Yield:7152-03-6 83%
Reaction Conditions:
with copper(II) ferrite in 1,2-dichloro-ethane at 35 - 38; for 18 h;Friedel-Crafts Acylation;
Steps:
General procedure: The FC acylation of various benzenes with acid chlorides was carried out in the presence of magnetic nano CuFe2O4 (particle size = 50 nm) by using one of the reaction condition (A-D) given below. Condition A: Anisole/arene (1 mmol), acid chloride (1.2 mmol), nano CuFe2O4 (20 mol %), 1,2-DCE (2 mL), 80 C and 24 h. Condition B: Anisole/arene (1 mmol), acid chloride (1.2 mmol), nano CuFe2O4 (20 mol %), 1,2-DCE (2 mL), rt (35-38 C) and 18 h. Condition C: Neat reaction, anisole/arene (3.3 mmol), acid chloride (1.2 mmol), nano CuFe2O4 (20 mol %), rt (35-38 C) and 18 h. Condition D: Neat reaction, arene/anisole (3.3 mmol), acid chloride (1.2 mmol), nano CuFe2O4 (20 mol %), 80 C and 18 h.
References:
Parella, Ramarao;Naveen;Kumar, Amit;Babu, Srinivasarao Arulananda [Tetrahedron Letters,2013,vol. 54,# 13,p. 1738 - 1742]
40877-19-8
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$24.89/5g
7152-03-6
94 suppliers
$15.00/5 g
100-66-3
541 suppliers
$10.00/5G
1759-53-1
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$6.00/10g
7152-03-6
94 suppliers
$15.00/5 g
3874-54-2
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$10.00/5 g
772-31-6
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$16.00/250mg
7152-03-6
94 suppliers
$15.00/5 g
104-92-7
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$10.00/10g
4023-34-1
371 suppliers
$12.00/5g
7152-03-6
94 suppliers
$15.00/5 g