DIETHYL-3-BUTENYLPHOSPHONATE 95 synthesis

8synthesis methods

10419-77-9 Synthesis

24850-33-7 Synthesis

Yield:15916-48-0 88%

Reaction Conditions:

with 2,2'-azobis(isobutyronitrile) in acetonitrile at 80; for 4 h;Inert atmosphere;

References:

Suzuki, Itaru;Kiyokawa, Kensuke;Yasuda, Makoto;Baba, Akio [Organic Letters,2013,vol. 15,# 7,p. 1728 - 1731] Location in patent:supporting information

106-95-6 Synthesis

10419-77-9 Synthesis

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