DIMETHYL TRIMETHYLSILYLMETHYLPHOSPHONATE synthesis
- Product Name:DIMETHYL TRIMETHYLSILYLMETHYLPHOSPHONATE
- CAS Number:13433-42-6
- Molecular formula:C6H17O3PSi
- Molecular Weight:196.26
Yield: 66%
Reaction Conditions:
Stage #1:dimethyl methane phosphonate with n-butyllithium;diisopropylamine in tetrahydrofuran;hexane at -78; for 0.333333 h;
Stage #2:chloro-trimethyl-silane in tetrahydrofuran;hexane at -78 - 30; for 0.5 h;
References:
Specklin, Simon;Cossy, Janine [Journal of Organic Chemistry,2015,vol. 80,# 6,p. 3302 - 3308]
![Phosphonic dichloride, [(trimethylsilyl)methyl]-](/CAS/20180601/GIF/13433-51-7.gif)
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