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ChemicalBook CAS DataBase List Glycitein

Glycitein synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: H2O2; SeO2 / CH2Cl2 / 16 h / 20 °C
2.1: 4.7818 g / aq. K2CO3 / methanol / 1 h / 20 °C
3.1: 77 percent / BF3*Et2O / 0.17 h / Heating
4.1: 0.01 h / microwave irradiation
4.2: 26 percent / methanesulfonyl chloride / 0.02 h / microwave irradiation

References:

Lang'at-Thoruwa, Caroline;Song, Tong T.;Hu, Jiang;Simons, Andrean L.;Murphy, Patricia A. [Journal of Natural Products,2003,vol. 66,# 1,p. 149 - 151]

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