ChemicalBook CAS DataBase List Boc-D-Ser(Bzl)-OH

Boc-D-Ser(Bzl)-OH synthesis

2synthesis methods

Product Name:Boc-D-Ser(Bzl)-OH
CAS Number:47173-80-8
Molecular formula:C15H21NO5
Molecular Weight:295.33

N-Boc D-Se (500 mg, 2.43 mmol) dissolved in anhydrous DMF (4 mL) was slowly added to a dispersion of 60% NaH (204 mg, 5.1 mmol) in anhydrous DMF at 0 ° C. Stir the mixture at room temperature for 1 hour and cool to 0 ° C. Subsequently, benzyl bromide (0.29 mL, 2.43 mmol) was added and the mixture was heated to room temperature. After 4 hours of reaction, add saturated NH4Cl (1 mL) to quench the reaction. Finally, the product Boc-D-Ser(Bzl)-OH was obtained through purification.

24424-99-5 Synthesis

24424-99-5
810 suppliers
$13.50/25G

47173-80-8
251 suppliers
$8.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium hydrogencarbonate; sodium carbonate / water
2: sodium hydride / N,N-dimethyl-formamide / 5 h / -40 °C

References:

Qi, Xian Liang;Yang, Er Qun;Zhang, Jun Tao;Wang, Tao;Cao, Xiao Ping [Chinese Chemical Letters,2012,vol. 23,# 6,p. 661 - 664]

FullText

24424-99-5 Synthesis

24424-99-5
810 suppliers
$13.50/25G

10433-52-0 Synthesis

10433-52-0
160 suppliers
$8.00/250mg

47173-80-8
251 suppliers
$8.00/1g

References

Boc-D-Ser(Bzl)-OH Related Search:

tert-Butanol L-Homoserine Benzyl benzoate D-Serine Benzyl chloride Benzyl alcohol Benzyltriethylammonium chloride DL-Serine Benzyltrimethylammonium chloride D-Cycloserine