?4-Chlorophenoxyacetic acid sodium salt synthesis
- Product Name:?4-Chlorophenoxyacetic acid sodium salt
- CAS Number:13730-98-8
- Molecular formula:C8H6ClNaO3
- Molecular Weight:208.57
4841-22-9
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$19.00/100mg
13730-98-8
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$59.00/5g
Yield:13730-98-8 209.15 g
Reaction Conditions:
with sodium hydrogencarbonate in water at 80; for 2 h;
Steps:
8
To the obtained methyl 4-chlorophenoxyacetate, 87.07 g of 99% sodium hydrogencarbonate and 129.30 g of water were added, and the mixture was reacted at 80 ° C for 2 h.At the same time, the alcohol formed by the reaction is distilled off, and the reaction is cooled down to room temperature for filtration.The filter cake is dried to obtain 209.15 g of sodium 4-chlorophenoxyacetate, and the content is 98.6%.The total yield was 98.86% based on phenol.
References:
Shandong Runbo Biological Technology Co., Ltd.;Sun Guoqing;Hou Yongsheng;Zhang Liguo;Chi Zhilong;Hu Yishan CN108947811, 2018, A Location in patent:Paragraph 0099; 0102
1892-43-9
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$17.67/1gm:
13730-98-8
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$59.00/5g
108-95-2
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$14.00/25g
13730-98-8
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2065-23-8
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$8.00/10g
13730-98-8
170 suppliers
$59.00/5g