Tris(tribromoneopenthyl)phosphate synthesis
- Product Name:Tris(tribromoneopenthyl)phosphate
- CAS Number:19186-97-1
- Molecular formula:C15H24Br9O4P
- Molecular Weight:1018.46
1522-92-5
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$6.00/25g
19186-97-1
156 suppliers
$45.00/1g
Yield:19186-97-1 83%
Reaction Conditions:
with magnesium chloride;trichlorophosphate in 1,1,2,2-tetrachloroethylene
Steps:
4 EXAMPLE 4
EXAMPLE 4 Following the procedures outlined in Example 1, 150 g of 3-bromo-2,2 bis(bromomethyl)propyl alcohol, 3 g anhydrous magnesium chloride and 25 g phosphorus oxychloride were mixed in 300 ml tetrachloroethylene in a flask. The contents were heated at reflux temperature for 21 hours. Following the described cooling, filtering and drying, a dry white product of 130 g of tris(3-bromo-2,2 bis(bromomethyl)propyl) phosphate was obtained, making an 83 percent yield based on the tribromoneopentyl alcohol.
References:
The Dow Chemical Company US4714771, 1987, A
115-77-5
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$10.00/10 g
19186-97-1
156 suppliers
$45.00/1g