1-Propanol synthesis
- Product Name:1-Propanol
- CAS Number:71-23-8
- Molecular formula:C3H8O
- Molecular Weight:60.1
123-38-6
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71-23-8
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Yield:71-23-8 100%
Reaction Conditions:
with hydrogen in water at 60; under 15001.5 Torr; for 8 h;Autoclave;Reagent/catalyst;
Steps:
2
General procedure: in25 mL of the autoclave was added0.5 mmol of different reactants, 50 mg of Co / ZrO2 La2O3 as catalyst,Add 10mL of deionized water, pass 2MPa hydrogen, heated to 60 , stirring conditions, the reaction after 8 hours,Cooling, deflating, and transferring the reaction solution with ethanol. After centrifugation, the catalyst and the reaction solution were separated and analyzed by gas chromatography.Gas chromatographic conditions are as follows: GC1690 gas chromatography, FID detector, capillary column (HP-5.30m × 0.250mm × 0.25μm), take the program temperature, the starting column temperature is 40 ,And the temperature was raised to 250 ° C for 3 minutes at a rate of 10 ° C / min. Carrier gas is 99.99% high purity nitrogen,The flow rate was 1 mL / min.
References:
CN107011107,2017,A Location in patent:Paragraph 0056-0061
57-55-6
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106-36-5
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71-23-8
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503-66-2
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71-23-8
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110-63-4
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71-23-8
745 suppliers
$12.00/100g