ChemicalBook--->CAS DataBase List--->22282-99-1

22282-99-1

22282-99-1 Structure

22282-99-1 Structure
IdentificationMore
[Name]

4-Bromo-2-methylpyridine
[CAS]

22282-99-1
[Synonyms]

2-METHYL-4-BROMOPYRIDINE
4-BROMO-2-METHYLPYRIDINE
4-BROMO-2-METHYL-PYRIDINE HYDROCHLORIDE
4-BROMO-2-METHYL-PYRIDINIUM, CHLORIDE
4-BROMO-2-PICOLINE
4-BROMO-2-PICOLINE HCL
4-BROMO-METHYL-PYRIDINE
CHEMBRDG-BB 4014101
2-Methyl-4-Bromopyridine HCl
4-BROMO-2-METHYLPYRIDINE 98%
4-BROMO-2-PICOLINE 4-BROMO-2-METHYLPYRIDINE
4-BROMO-2-METHYLPYRIDINE (4-BROMO-2-PICOLINE)
[EINECS(EC#)]

624-896-3
[Molecular Formula]

C6H6BrN
[MDL Number]

MFCD03788196
[Molecular Weight]

172.02
[MOL File]

22282-99-1.mol
Chemical PropertiesBack Directory
[Appearance]

Light yellow liquid
[Boiling point ]

76 °C / 14mmHg
[density ]

1.450 g/mL at 25 °C
[refractive index ]

n 20/D 1.556
[Fp ]

174 °F
[storage temp. ]

Inert atmosphere,2-8°C
[solubility ]

Dichloromethane
[form ]

Pale Yellow Liquid
[pka]

4.38±0.10(Predicted)
[Water Solubility ]

Miscible with dichloromethane. Immiscible with water.
[CAS DataBase Reference]

22282-99-1(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xn,Xi
[Risk Statements ]

R22:Harmful if swallowed.
R37/38:Irritating to respiratory system and skin .
R41:Risk of serious damage to eyes.
R36/37/38:Irritating to eyes, respiratory system and skin .
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/39:Wear suitable protective clothing and eye/face protection .
S36:Wear suitable protective clothing .
[RIDADR ]

NA 1993 / PGIII
[WGK Germany ]

3
[Hazard Note ]

Irritant
[HazardClass ]

IRRITANT
[HS Code ]

29333990
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Diethyl ether-->Sodium carbonate-->Chloroform-->Ammonium hydroxide-->Phosphorus trichloride-->4-Nitro-2-picoline N-oxide-->Acetyl bromide-->4-BROMOPYRIDINE-2-CARBALDEHYDE-->2-Picoline-N-oxide-->2-Chloro-4-nitropyridine-->2-Methyl-4-nitropyridine-->Methylmagnesium Bromide-->2,4-Dibromopyridine
[Preparation Products]

(4-METHOXY-PYRIDIN-2-YL)-METHANOL-->4-METHOXYPICOLINALDEHYDE-->4-BROMO-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER-->TERT-BUTYL 4-BROMOPYRIDIN-2-YLCARBAMATE-->2-METHYLPYRIDINE-4-BORONIC ACID PINACOL ESTER-->4-Bromo-2-pyridinemethanol
Hazard InformationBack Directory
[Chemical Properties]

Light yellow liquid
[Uses]

4-Bromo-2-methylpyridine is a starting material used in a synthesis of crown-ester-bipyridines and viologens via sodium or nickel reductive coupling, side chain oxidation and esterification.
[Uses]

4-Bromo-2-methylpyridine is used as a starting material in the preparation of crown-ester-bipyridines and viologens through sodium or nickel reductive coupling, side chain oxidation and esterification. Further, it serves as an important raw material and intermediate in organic synthesis, pharmaceuticals, agrochemicals and in dyes.
[Uses]

Used in the preparation of phenyloxadiazolyl pyridines as immunomodulating agents.
Spectrum DetailBack Directory
[Spectrum Detail]

4-Bromo-2-methylpyridine(22282-99-1)1HNMR
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

4-Bromo-2-methylpyridine, 97%(22282-99-1)
[Sigma Aldrich]

22282-99-1(sigmaaldrich)
[TCI AMERICA]

4-Bromo-2-picoline,>98.0%(GC)(T)(22282-99-1)
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