ChemicalBook--->CAS DataBase List--->4156-16-5

4156-16-5

4156-16-5 Structure

4156-16-5 Structure
IdentificationMore
[Name]

2-Ethyl-5-phenylisoxazolium-3'-sulfonate
[CAS]

4156-16-5
[Synonyms]

2-ETHYL-5-PHENYLISOXAZOLIUM-3'-SULFONATE
2-ETHYL-5-PHENYLISOXAZOLIUM-3'-SULPHONATE
3-(2-ETHYL-5-ISOXAZOLIO)BENZENESULFONATE
NEPIS
N-ETHYL-5-PHENYLISOXAZOLIUM-3'-SULFONATE
WOODWARDS REAGENT K
WOODWARD'S REAGENT K
3-(2-Ethyl-5-isoxazolio)benzenesulphonate~NEPIS~Woodwards
2-ETHYL-5-PHENYLISOXAZOLIUM-3'-SULPHONEATE
Isoxazolium, 2-ethyl-5-(3-sulfophenyl)-, inner salt
NEPIS 2-ETHYL-5-PHENYLISOXAZOLIUM-3''-SULFONATE
3-(2-ETHYL-5-ISOXAZOLIO)BENZENESULFONATE 99+%
2-Ethyl-5-phenylisoxazolium-3μ-sulfonate, NEPIS
5-(3-Sulfonatophenyl)-2-ethylisoxazol-2-ium
[EINECS(EC#)]

223-988-7
[Molecular Formula]

C11H11NO4S
[MDL Number]

MFCD00012128
[Molecular Weight]

253.27
[MOL File]

4156-16-5.mol
Chemical PropertiesBack Directory
[Appearance]

white to off-white crystalline powder
[Melting point ]

216-219 °C (dec.)
[density ]

1.3854 (rough estimate)
[refractive index ]

1.4790 (estimate)
[storage temp. ]

Store at RT.
[Merck ]

10050
[BRN ]

4149224
[CAS DataBase Reference]

4156-16-5(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xn
[Risk Statements ]

22
[WGK Germany ]

3
Hazard InformationBack Directory
[Chemical Properties]

white to off-white crystalline powder
[Uses]

Peptide-bond former.
[Purification Methods]

Crystallise the reagent from diethyl ether or ethyl acetate/pet ether. [Lamas et al. J Am Chem Soc 108 5543 1986.] It is best purified by dissolving in excess of aqueous N HCl and precipitating with Me2CO to give a white fluffy solid. [Woodward et al. Tetrahedron 22 Suppl 8 321 1966, Fieser & Fieser Reagents for Organic Synthesis 1 385, 2 198.]
Spectrum DetailBack Directory
[Spectrum Detail]

2-Ethyl-5-phenylisoxazolium-3'-sulfonate(4156-16-5)1HNMR
2-Ethyl-5-phenylisoxazolium-3'-sulfonate(4156-16-5)IR1
2-Ethyl-5-phenylisoxazolium-3'-sulfonate(4156-16-5)Raman
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

4156-16-5(sigmaaldrich)
[TCI AMERICA]

N-Ethyl-5-phenylisoxazolium-3'-sulfonate,>98.0%(T)(4156-16-5)
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