| Identification | More | [Name]
Methyl 2-bromobenzoate | [CAS]
610-94-6 | [Synonyms]
2-BROMOBENZOIC ACID METHYL ESTER
METHYL 2-BROMOBENZOATE
METHYL O-BROMOBENZOATE
RARECHEM AL BF 0014
2-bromo-benzoicacimethylester
Benzoicacid,2-bromo-,methylester
O-bromobenzoic acid, methyl ester
Methyl2-bromobenzoate,99%
2-(Methoxycarbonyl)-1-bromobenzene | [EINECS(EC#)]
210-241-5 | [Molecular Formula]
C8H7BrO2 | [MDL Number]
MFCD00016328 | [Molecular Weight]
215.04 | [MOL File]
610-94-6.mol |
| Hazard Information | Back Directory | [Chemical Properties]
CLEAR LIGHT YELLOW LIQUID | [Uses]
Methyl 2-bromobenzoate under Heck reaction with acrylonitrile results in lactonization to give the benzofuran-2-one 3-(cyanomethyl)-2-coumaranone. It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals | [Synthesis]
Preparation of methyl o-bromobenzoate: In a 250 ml three-necked flask, add 0.04 mol of methyl benzoate and 100 ml of acetic acid, stir to dissolve, and then cool to 0 °C using an ice-salt bath. Dissolve 0.05 mol of Br2 in 50 ml of acetic acid, and slow | [Purification Methods]
A solution of the ester in ether is washed with 10% aqueous Na 2CO3, water, then dried and distilled. [Beilstein 9 |
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