1-Methyl-3-pyrrolidinol
- CAS No.
- 13220-33-2
- Chemical Name:
- 1-Methyl-3-pyrrolidinol
- Synonyms
- 1-METHYL-PYRROLIDIN-3-OL;3-HYDROXY-1-METHYLPYRROLIDINE;NSC 89279;3-Hydroxy-1-methyL;N-Methyl-3-hydroxy-;1-Methyl-3-pyrrolidi;N-methyl-3-pyrrolitol;N-Methyl-3-pyrrolidinol;1-METHYL-3-PYRROLIDINOL;N-Methyl-pyrrolidin-3-ol
- CBNumber:
- CB9296691
- Molecular Formula:
- C5H11NO
- Molecular Weight:
- 101.15
- MDL Number:
- MFCD00003176
- MOL File:
- 13220-33-2.mol
- MSDS File:
- SDS
Boiling point | 50-52 °C1 mm Hg(lit.) |
---|---|
Density | 0.921 g/mL at 25 °C(lit.) |
refractive index |
n |
Flash point | 159 °F |
storage temp. | 2-8°C |
solubility | Chloroform (Slightly), Methanol (Slightly) |
form | Oil |
pka | 14.95±0.20(Predicted) |
color | Colourless |
InChI | InChI=1S/C5H11NO/c1-6-3-2-5(7)4-6/h5,7H,2-4H2,1H3 |
InChIKey | FLVFPAIGVBQGET-UHFFFAOYSA-N |
SMILES | N1(C)CCC(O)C1 |
CAS DataBase Reference | 13220-33-2(CAS DataBase Reference) |
FDA UNII | CGW2AL7PQ7 |
NIST Chemistry Reference | 1-Methyl-3-pyrrolidinol(13220-33-2) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
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Signal word | Warning | |||||||||
Hazard statements | H227-H315-H319-H335 | |||||||||
Precautionary statements | P210e-P261-P280a-P305+P351+P338-P405-P501a | |||||||||
Hazard Codes | Xi | |||||||||
Risk Statements | 36/37/38 | |||||||||
Safety Statements | 26-36/37/39 | |||||||||
WGK Germany | 3 | |||||||||
HS Code | 29339900 | |||||||||
NFPA 704 |
|
1-Methyl-3-pyrrolidinol price More Price(35)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich | M79506 | 1-Methyl-3-pyrrolidinol 95% | 13220-33-2 | 1g | $41.7 | 2024-03-01 | Buy |
TCI Chemical | M2115 | 1-Methyl-3-pyrrolidinol | 13220-33-2 | 5G | $100 | 2024-03-01 | Buy |
TCI Chemical | M2115 | 1-Methyl-3-pyrrolidinol | 13220-33-2 | 25G | $347 | 2024-03-01 | Buy |
Alfa Aesar | H28122 | 3-Hydroxy-1-methylpyrrolidine, 97% | 13220-33-2 | 1g | $93.9 | 2023-06-20 | Buy |
Alfa Aesar | H28122 | 3-Hydroxy-1-methylpyrrolidine, 97% | 13220-33-2 | 5g | $307 | 2023-06-20 | Buy |
1-Methyl-3-pyrrolidinol Chemical Properties,Uses,Production
Chemical Properties
Clear colorless to pale yellow liquid
Uses
1-Methyl-3-pyrrolidinol (cas# 13220-33-2) is a compound useful in organic synthesis.
Synthesis
A 500 mL four-necked flask was charged with a 40 wt% aqueous solution of monomethylamine and cooled to 10 ° C in an ice-water bath. Then, while stirring, 1,4-dichloro-2-butanol was added dropwise, and the temperature was controlled at 15 ° C. Then pour the system into an Autoclave, sealed, evacuated to a pressure of 1.0 ± 0.1MPa, while heated to 120 ℃, the reaction was stirred for about 10h. After the reaction was over and cooled to room temperature, the material was discharged, batch-wise added sodium hydroxide was released, and a large amount of methylamine gas, controlling the temperature below 50 ℃, precipitated a lot of white solid, stirred for 1h; filtration, the filtrate layered, the upper organic phase Ethanol And anhydrous magnesium sulfate, stirring 2 ~ 3h; and then filtered, the filtrate was concentrated in vacuo to give a yellow transparent oily liquid, and then vacuum distillation to give colorless and t1-Methyl-3-pyrrolidinol, Yield 64.8%, purity 99.3%.
1-Methyl-3-pyrrolidinol Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Anhui Dexinjia Biopharm Co., Ltd | +86-531-82375818 +8615064153060 | sales01@jndxj.com | China | 291 | 58 |
Hebei Mojin Biotechnology Co., Ltd | +86 13288715578 +8613288715578 | sales@hbmojin.com | China | 12446 | 58 |
Zibo Hangyu Biotechnology Development Co., Ltd | +86-0533-2185556 +8617865335152 | Mandy@hangyubiotech.com | China | 10991 | 58 |
Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 | sales@capotchem.com | China | 29798 | 60 |
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 18628 | 58 |
Beijing Cooperate Pharmaceutical Co.,Ltd | 010-60279497 | sales01@cooperate-pharm.com | CHINA | 1811 | 55 |
Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | info@tianfuchem.com | China | 21667 | 55 |
career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29888 | 58 |
Zhejiang ZETian Fine Chemicals Co. LTD | +8618957127338 | stella@zetchem.com | China | 2136 | 58 |
Accela ChemBio Inc. | +1-858-6993322 | info@accelachem.com | United States | 19536 | 58 |
View Lastest Price from 1-Methyl-3-pyrrolidinol manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2024-09-02 | 1-Methyl-3-pyrrolidinol
13220-33-2
|
US $200.00-4000.00 / KG | 100g | no less than 98% | 1MT per month | Anhui Dexinjia Biopharm Co., Ltd | ||
2024-08-29 | 1-Methyl-3-pyrrolidinol
13220-33-2
|
US $3360.00-3310.00 / kg | 200kg | 99.99% | 100Tons | Hebei Dangtong Import and export Co LTD | ||
2024-08-27 | 1-Methyl-3-pyrrolidinol
13220-33-2
|
US $80.00-800.00 / kg | 10kg | 0.99 | 20tons | Zibo Hangyu Biotechnology Development Co., Ltd |
- 1-Methyl-3-pyrrolidinol
13220-33-2
- US $200.00-4000.00 / KG
- no less than 98%
- Anhui Dexinjia Biopharm Co., Ltd
- 1-Methyl-3-pyrrolidinol
13220-33-2
- US $3360.00-3310.00 / kg
- 99.99%
- Hebei Dangtong Import and export Co LTD
- 1-Methyl-3-pyrrolidinol
13220-33-2
- US $80.00-800.00 / kg
- 0.99
- Zibo Hangyu Biotechnology Development Co., Ltd