2,4-Hexadienal synthesis
- Product Name:2,4-Hexadienal
- CAS Number:80466-34-8
- Molecular formula:C6H8O
- Molecular Weight:96.13
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Yield: 22% ， 14% ， 7% ， 6%
Reaction Conditions:
with N-(benzoyl)-L-proline in N,N-dimethyl acetamide at 125; for 3 h;Autoclave;Aldol Condensation;
Steps:
General procedure: The experiments were carried out in static steel and glass thick-walled autoclaves (Aldrich) at 25 and 125°C for 3 and 24 h, respectively. Water, toluene, N,N'-dimethylacetamide (DMAA) were used as a solvent. A weighed amount of a solvent was placed into the autoclave, a required amount of an aldehyde was added, and a catalyst was introduced into the obtained solution. The process is accompanied by the change in the color of the reaction solution from pale yellow to black depending on the catalytic system used.
References:
Martsinkevich;Bruk;Dashko;Afaunov;Flid;Sedov [Petroleum Chemistry,2018,vol. 58,# 12,p. 1032 - 1035][Neftekhimiya,2018,vol. 58,# 6,p. 686 - 689,4]
50-00-0
897 suppliers
$10.00/25g
75-07-0
431 suppliers
$14.00/5mL
80466-34-8
17 suppliers
inquiry
107-02-8
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$38.60/4s8501
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$40.00/5g
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80466-34-8
17 suppliers
inquiry
75-07-0
431 suppliers
$14.00/5mL
123-73-9
236 suppliers
$40.00/5g
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
