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ChemicalBook CAS DataBase List (3-BROMOPROPOXY)-TERT-BUTYLDIMETHYLSILANE
59501-41-6

(3-BROMOPROPOXY)-TERT-BUTYLDIMETHYLSILANE synthesis

8synthesis methods
-

Yield:3739-67-1 51%

Reaction Conditions:

Stage #1: BPAwith chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II);silver(I) 4-methylbenzenesulfonate;toluene-4-sulfonic acid in toluene; for 0.0833333 h;Inert atmosphere;
Stage #2: Allyl ether in toluene at 60; for 3 h;Inert atmosphere;

References:

Van Rijn, Jimmy A.;Guijt, Marieke C.;Bouwman, Elisabeth;Drent, Eite [Applied Organometallic Chemistry,2011,vol. 25,# 3,p. 207 - 211] Location in patent:experimental part