4-METHOXY-3-PROPOXYBENZALDEHYDE synthesis
- Product Name:4-METHOXY-3-PROPOXYBENZALDEHYDE
- CAS Number:5922-56-5
- Molecular formula:C11H14O3
- Molecular Weight:194.23
621-59-0
653 suppliers
$9.00/1g
107-08-4
256 suppliers
$14.00/5g
5922-56-5
22 suppliers
$60.00/100mg
Yield:5922-56-5 99%
Reaction Conditions:
with potassium carbonate;potassium iodide in butanone;Reflux;
Steps:
Synthesis of Table 1 Molecule Number 29, 30 & 39
Synthesis of Table 1 Molecule Number 29, 30 & 39 _:To a solution of iso- vanillin (1 eq.) in MEK (0.5 M) was added n-Prl (1.1 eq.), potassium carbonate (3 eq.) and potassium iodide (1 %). The resulting mixture was heated to reflux temperature and stirred overnight. The reaction was concentrated under reduced pressure, quenched by addition of a saturated NH4C1 aqueous solution and extracted with Et20. The combined organic layers were dried over MgS04and concentrated under reduced pressure. The resulting oil was purified using a quick filtration over silica by elution with a petroleum ether- Et20 mixture (9-1). Concentration of the eluent under reduced pressure resulted in the compound as a colorless oil (99% yield).
References:
WO2015/148743,2015,A1 Location in patent:Page/Page column 67
621-59-0
653 suppliers
$9.00/1g
106-94-5
582 suppliers
$10.00/5ml
5922-56-5
22 suppliers
$60.00/100mg
110943-74-3
1 suppliers
inquiry
77-78-1
323 suppliers
$22.00/25g
5922-56-5
22 suppliers
$60.00/100mg
621-59-0
653 suppliers
$9.00/1g
5922-56-5
22 suppliers
$60.00/100mg
2973-78-6
221 suppliers
$14.00/5g
5922-56-5
22 suppliers
$60.00/100mg