N,N'-diethyl-N,N'-diphenylthioperoxydicarbamic acid synthesis
- Product Name:N,N'-diethyl-N,N'-diphenylthioperoxydicarbamic acid
- CAS Number:41365-24-6
- Molecular formula:C18H20N2S4
- Molecular Weight:392.61
75-15-0
266 suppliers
$40.00/100g
103-69-5
273 suppliers
$13.00/100g
41365-24-6
18 suppliers
inquiry
Yield:41365-24-6 98.9%
Reaction Conditions:
with pyridine;dihydrogen peroxide in cyclohexane at 0 - 10; for 6 h;
Steps:
2 Example 2
200mL cyclohexane, 32.1g carbon disulfide, 45.2g N-ethylaniline,0.04g pyridine was added to the 1L flask and stirred; at 010,Slowly add 127.0g of 5% hydrogen peroxide, and finish after 6h; keep warm,TLC followed until the end of the reaction. Suction filtration gave white N,N'-diethyl-N,N'-diphenylthiuram disulfide. The yield is 98.9%,The purity by HPLC was 98.9%.
References:
CN111116439,2020,A Location in patent:Paragraph 0024-0025
13074-29-8
0 suppliers
inquiry
41365-24-6
18 suppliers
inquiry
103-69-5
273 suppliers
$13.00/100g
41365-24-6
18 suppliers
inquiry
110-86-1
884 suppliers
$9.00/5g
75-15-0
266 suppliers
$40.00/100g
7553-56-2
652 suppliers
$20.69/25G
103-69-5
273 suppliers
$13.00/100g
41365-24-6
18 suppliers
inquiry