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19164-61-5

7-phenylbicyclo[4.2.0]octa-1,3,5-trien-7-ol synthesis

7synthesis methods
-

Yield:19164-61-5 35%

Reaction Conditions:

Stage #1: acetophenonewith tetramethylpiperidine;tert.-butyl lithium in tetrahydrofuran;hexane at -40;
Stage #2: chlorobenzene in tetrahydrofuran;hexane at -40; for 5 h;

References:

Tripathy, Sasmita;Reddy, Ranga;Durst, Tony [Canadian Journal of Chemistry,2003,vol. 81,# 9,p. 997 - 1002]