ETHYL 2-METHYLBENZOYLFORMATE synthesis
- Product Name:ETHYL 2-METHYLBENZOYLFORMATE
- CAS Number:66644-67-5
- Molecular formula:C11H12O3
- Molecular Weight:192.21
95-49-8
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4755-77-5
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66644-67-5
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$220.00/200mg
Yield:66644-67-5 91%
Reaction Conditions:
Stage #1: 2-methylchlorobenzenewith lithium in diethyl ether at 3 - 6;
Stage #2: with copper(l) cyanide in tetrahydrofuran;diethyl ether at 3 - 6; for 0.416667 h;Cooling with ice;
Stage #3: Ethyl oxalyl chloride in tetrahydrofuran;diethyl ether at 3 - 20; for 1.25 h;
References:
Screttas, Constantinos G.;Steele, Barry R.;Micha-Screttas, Maria;Heropoulos, Georgios A. [Organic Letters,2012,vol. 14,# 22,p. 5680 - 5683] Location in patent:supporting information
40291-39-2
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66644-67-5
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$220.00/200mg
95-46-5
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95-92-1
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66644-67-5
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16419-60-6
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623-49-4
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66644-67-5
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$220.00/200mg
35276-81-4
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64-17-5
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66644-67-5
19 suppliers
$220.00/200mg