Ethyl ethoxyacetate synthesis
- Product Name:Ethyl ethoxyacetate
- CAS Number:817-95-8
- Molecular formula:C6H12O3
- Molecular Weight:132.16
64-17-5
846 suppliers
$10.00/50g
627-03-2
177 suppliers
$21.21/5gm:
817-95-8
164 suppliers
$49.00/5g
Yield:817-95-8 78%
Reaction Conditions:
with sulfuric acid at 100; for 2 h;Inert atmosphere;
Steps:
171.a Preparation of 2-ethoxyethyl acetate
Is set to have a 2-ethoxyacetic acid (20g, 0.19mol) in ethanol (200 mL) was added sulfuric acid (10mL). The resultant reactionmixture was reacted at 100 degrees for two hours. After completion of the reaction, the reaction solution was diluted with ethylacetate and after concentrating, the organic phase was washed twice with water, dried over anhydrous sodium sulfate andconcentrated to a yellow oily liquid (19.5g, 78%).
References:
MEDSHINEDISCOVERY INC.;CHENXIN PHARMACEUTICAL LTD;Zheng, Huiping;Wu, Chengde;Yu, Tao;Huang, Lei;Hao, Dongling;Gao, Bo;Sun, Jikui;Shi, Nengyang;Chen, Shuhui TW2016/2107, 2016, A Location in patent:Paragraph 0106; 0107
623-73-4
139 suppliers
$26.69/5g
64-17-5
846 suppliers
$10.00/50g
817-95-8
164 suppliers
$49.00/5g
1520-50-9
0 suppliers
inquiry
6065-82-3
214 suppliers
$5.00/1g
817-95-8
164 suppliers
$49.00/5g