ChemicalBook CAS DataBase List Ethyl tiglate

Ethyl tiglate synthesis

7synthesis methods

Product Name:Ethyl tiglate
CAS Number:5837-78-5
Molecular formula:C7H12O2
Molecular Weight:128.17

By direct esterification of tiglic acid with ethyl alcohol in the presence of concentrated H2SO4 or by reaction of bromomethylethyl acetic acid ethyl ester with dimethylaniline.

105-37-3 Synthesis

105-37-3
375 suppliers
$10.00/5mL

5837-78-5
131 suppliers
$14.00/1g

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) diisopropylamine, n-butyllithium / 1.) THF, hexane, -78 deg C, 30 min; 2.) -78 deg C, 15 min; room temp., 1 h
2: butyllithium / hexane; diethyl ether / -40 - -30 °C
3: triethylamine / methanol / 6 h / Heating

References:

Slougui, Nasser;Rousseau, Gerard;Conia, Jean-Marie [Synthesis,1982,# 1,p. 58 - 60]

80-59-1 Synthesis

80-59-1
310 suppliers
$5.00/250mg

64-17-5 Synthesis

64-17-5
693 suppliers
$10.00/50g

5837-78-5
131 suppliers
$14.00/1g

References

547-65-9 Synthesis

547-65-9
155 suppliers
$48.00/1g

64-17-5 Synthesis

64-17-5
693 suppliers
$10.00/50g

22122-36-7 Synthesis

22122-36-7
75 suppliers
$45.00/50mg

5837-78-5
131 suppliers
$14.00/1g

References

Silane, [(1-ethoxy-1-propenyl)oxy]trimethyl-

80675-53-2
0 suppliers
inquiry

5837-78-5
131 suppliers
$14.00/1g

References

609-14-3 Synthesis

609-14-3
270 suppliers
$5.00/5g

5837-78-5
131 suppliers
$14.00/1g

References

Ethyl tiglate Related Search:

2-Methyl-2-butene Maleic acid Ethyl acetate Fumaric acid Ethanol Methylparaben Diethyl succinosuccinate 2-Hydroxyethyl methacrylate Methyl acetate 5-Chlorovaleric acid