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ChemicalBook CAS DataBase List N-(2-NAPHTHYL)FORMAMIDE 97
4423-74-9

N-(2-NAPHTHYL)FORMAMIDE 97 synthesis

12synthesis methods
-

Yield:4423-74-9 99%

Reaction Conditions:

with sulfonic acid and propylamine functionalized HY zeolite in neat (no solvent) at 20; for 0.116667 h;Green chemistry;

Steps:

General procedure for formylation of amines

General procedure: (1.2 mmol) Formic acid was added to a mixture of aniline(1 mmol) and catalyst (0.02 g). This mixture was stirredat room temperature for the appropriate time and the progressof reaction followed by TLC. After completion reaction,products extracted by 4 mL of ethanol and chloroformmixture and catalyst filtrated, washed and dried for reuse.The structures of the products were established from theirphysical properties and spectral (1H NMR, 13C NMR andFT-IR) analysis and compared with the data that reportedin the literature.

References:

Zendehdel, Mojgan;Tavakoli, Fatemeh [Journal of the Iranian Chemical Society,2022,vol. 19,# 4,p. 1095 - 1107]