SALICYLIDENE 2-AMINOPYRIDINE synthesis
- Product Name:SALICYLIDENE 2-AMINOPYRIDINE
- CAS Number:1823-47-8
- Molecular formula:C12H10N2O
- Molecular Weight:198.22
Yield:1823-47-8 96%
Reaction Conditions:
in neat (no solvent) at 20; for 0.166667 h;Green chemistry;
Steps:
Preparation of azomethines (entries 1-15):
General procedure: A mixture of 2-aminopyridine (1 mmol) and appropriate aromatic aldehyde (1 mmol) was ground thoroughly in a clean, dry porcelain mortar with a pestle until the mixture became sticky. The sticky mass was left in air for 2-70 min (Table 1) with a little grinding from time to time. When the reaction was completed (as indicated by TLC), the solid mass was taken out of the inner wall of the morter with the flat end of a spatula. All the compounds were recrystallised from dilute aqueous ethanol.
References:
Sarma, Madhushree Das;Ghosh, Subhojit [Journal of the Indian Chemical Society,2020,vol. 97,# 8,p. 1295 - 1303]
504-29-0
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1823-47-8
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$28.60/250MG
110-86-1
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1823-47-8
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1823-47-8
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$28.60/250MG