ChemicalBook--->CAS DataBase List--->40258-78-4

40258-78-4

40258-78-4 Structure

40258-78-4 Structure
IdentificationBack Directory
[Name]

1-Bromoethyl acetate
[CAS]

40258-78-4
[Synonyms]

1-BROMOETHYLACETATE
Cefuroxime Impurity 51
1-ACETOXY ETHYL BROMIDE
Theophylline Impurity 10
1-Bromoethyl acetate ,90%
1 - broMine ethyl acetate
1-Bromoethyl acetate[BEA]
(RS)-1-Acetoxyethyl BroMide
Ethanol, 1-bromo-, 1-acetate
1‐Acetoxy?Ethyl?Bromide?(1‐AEB)
1-Acetoxy Ethyl Bromide (1-AEB) CAS No. : 40258-78-4
[EINECS(EC#)]

609-807-8
[Molecular Formula]

C4H7BrO2
[MDL Number]

MFCD08061392
[MOL File]

40258-78-4.mol
[Molecular Weight]

167
Chemical PropertiesBack Directory
[Boiling point ]

122-125 °C(Press: 738 Torr)
[density ]

1.48
[storage temp. ]

Inert atmosphere,2-8°C
Safety DataBack Directory
[Symbol(GHS) ]


GHS02,GHS07
[Signal word ]

Warning
[Hazard statements ]

H335-H226-H315-H319
[Precautionary statements ]

P264-P280-P305+P351+P338-P337+P313P-P264-P280-P302+P352-P321-P332+P313-P362
[Safety Statements ]

24/25
[HS Code ]

29153900
Hazard InformationBack Directory
[Chemical Properties]

Pale Yellow Oil
[Uses]

1-Bromoethyl Acetate is a 1-haloalkyl ester that is used in the modification of of antibiotics.
[Synthesis]

1-bromoethyl acetate is prepared by reacting acetyl bromide and acetaldehyde using zinc chloride as a catalyst. 
After cooling 30 ml of hydrogen bromide / acetic acid (1.2 equiv) to 0 ° C., 53.5 ml (1.0 equiv) of vinyl acetate was slowly added thereto, followed by stirring for 1 hour. It was extracted with dichloromethane, washed with distilled water at 0-5 ° C., dehydrated with anhydrous magnesium sulfate, and distilled under reduced pressure to obtain 81.4 g of 1-bromoethyl acetate.
synthesis of 1-bromoethyl acetate
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