ChemicalBook CAS DataBase List Benzaldehyde, 4-(ethylamino)- (9CI)

Benzaldehyde, 4-(ethylamino)- (9CI) synthesis

9synthesis methods

Product Name:Benzaldehyde, 4-(ethylamino)- (9CI)
CAS Number:79865-89-7
Molecular formula:C9H11NO
Molecular Weight:149.19

64-17-5 Synthesis

64-17-5
700 suppliers
$10.00/50g

555-16-8
527 suppliers
$5.00/5g

79865-89-7
50 suppliers
$53.00/100mg

Yield:79865-89-7 97.3%

Reaction Conditions:

with hydrogen in ethanol at 160; under 15001.5 Torr; for 7 h;

Steps:

2.5 Catalytic reactions and product analysis

The nitroarenes (0.81mmol), alcohols and the as-synthesized catalysts were placed in reactor (100mL). Before hydrogenation-alkylation tandem experiments, the reactor was purged with N₂ and H₂ to remove the air and N₂ for three times, respectively. The reaction mixture were isolated by the magnet, and the isolated NiCo/MgO-C catalyst was washed with ethanol and dried before reused for recyclability measurement. The conversions and yields of reactions of hydrogenation-alkylation tandem reaction were analyzed by using GC-MS.

References:

Li, Weizuo;Wang, Jing;He, Dafang;He, Guangyu;Chen, Haiqun [Molecular catalysis,2022,vol. 529,art. no. 112520]

459-57-4 Synthesis