Ethyl 2-(4-bromophenyl)-2-diazoacetate synthesis
- Product Name:Ethyl 2-(4-bromophenyl)-2-diazoacetate
- CAS Number:758692-47-6
- Molecular formula:C10H9BrN2O2
- Molecular Weight:269.09
20201-26-7
115 suppliers
$8.00/100mg
758692-47-6
22 suppliers
inquiry
Yield:758692-47-6 95%
Reaction Conditions:
Stage #1: ethyl 2-(4-bromophenyl)-2-oxoacetatewith benzoic acid;hydrazine in tetrahydrofuran at 20; for 16 h;
Stage #2: with potassium N-iodo p-toluenesulfonamide;potassium hydroxide in tetrahydrofuran;lithium hydroxide monohydrate at 20;
References:
Nicolle, Simon M.;Moody, Christopher J. [Chemistry - A European Journal,2014,vol. 20,# 15,p. 4420 - 4425] Location in patent:supporting information
14062-25-0
252 suppliers
$6.00/5g
758692-47-6
22 suppliers
inquiry
623-73-4
150 suppliers
$27.30/25ML
589-87-7
540 suppliers
$10.00/1g
758692-47-6
22 suppliers
inquiry
1878-68-8
500 suppliers
$6.00/10g
758692-47-6
22 suppliers
inquiry