Silane, chloro(4-chlorophenyl)dimethyl- synthesis
- Product Name:Silane, chloro(4-chlorophenyl)dimethyl-
- CAS Number:825-92-3
- Molecular formula:C8H10Cl2Si
- Molecular Weight:205.16
Yield:825-92-3 99.5%
Steps:
11 Example 11
Example 11 The same procedures used in Example 10 were repeated except that 170.7 g (1.0 mole) of p-chlorophenyldimethylsilane was substituted for 136.3 g of the dimethylphenylsilane used in Example 10 to carry out the reaction of the allyl chloride and the p-chlorophenyldimethylsilane. A distillate having a boiling point range of from 103 to 104° C./11 mmHg was recovered through distillation and thus 197.1 g of p-chlorophenyldimethylchlorosilane having a purity of 99.5% was obtained. The yield of the product was found to be 96.1%.
References:
US5342984,1994,A
4342-61-4
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122-01-0
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95-50-1
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825-92-3
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